This book is created to understand experiments of pharmaceutical organic chemistry-II as per PCI. It will helpful to students to learn the reaction, mechanism, procedure, calculation, result and uses of organic compound. This book correlates with theory of pharmaceutical organic chemistry II which been inserted in PCI syllabus of Second year B. Pharm Sem-III. This book covers easy ways methods to achieve precision and accuracy in practicals Book includes analysis of fats and oils like acid value, saponification value, iodine value determination. Book contains major experiments includes Synthesis and characterization of various organic compounds such as 2,4 6 tri-bromo aniline, meta dinitro benzene, benzoic acid, phenyl benzoate, dibenzal acetone, phenyl azo 2-naphthol, p-bromo acetanilide, para iodo benzoic acid, benzil and 9,10 anthraquinone. Purification and isolation of synthesized compounds were included like steam distillation and recrystalisation